In-situ Differential Electrochemical Mass Spectrometry (DEMS) for Battery Energy Storage Devices
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In-situ Differential Electrochemical Mass Spectrometry (DEMS) for Battery Energy Storage Devices
Introduction
The Differential Electrochemical Mass Spectrometry System is a state-of-the-art in-situ DEMS platform designed for advanced battery research and gas analysis. Engineered with a modular architecture and ultra-high sensitivity, this system enables real-time monitoring of gas generation and consumption during electrochemical reactions. It is especially well suited for studying lithium-ion, sodium-ion, metal-air, and Li-O2 battery systems, helping researchers gain deeper insight into electrode reactions, electrolyte decomposition, and battery failure mechanisms. The brochure presents the QAS100 Li as a turnkey DEMS solution for battery energy storage devices, with coupled electrochemical and mass spectrometry software for efficient testing and data processing.

Field-axis technology
Key Features
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Turnkey in-situ DEMS solution for battery gas analysis
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Modular design with wide battery application compatibility
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Ultra-high sensitivity and low detection limit down to 3 × 10^-15 mbar
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Supports lithium-ion, sodium-ion, metal-air, and Li-O2 batteries
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Dual carrier gas system for high sensitivity and flexible operation
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Compatible with coin cell and pouch cell modules
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Battery mold temperature control from RT to 100°C
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Coupled electrochemical workstation and mass spectrometry software for convenient data acquisition and processing
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Can be combined with in-situ Raman or in-situ XRD
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Swagelok battery module offers small head space volume, gas-tight sealing, and good reproducibility
Specification
| Model | QAS100 Li |
| Product Type | Differential Electrochemical Mass Spectrometry System |
| Mass Range | 1–100 / 1–200 / 1–300 amu |
| Detection Limit | 3 × 10^-15 mbar |
| Sensitivity | 5 × 10^-4 A/mbar |
| Fast Scanning Speed | 1 ms/amu |
| Detector | Electron Multiplier and Faraday |
| Software | PV MassSpec |
| Electron Energy Range | Up to 150 eV |
| Ion Source | EI |
| Filament Emission Current Range | 1–2000 μA |
| Vacuum System | Turbo pump |
| Ultimate Pressure | 1 × 10^-7 mbar |
| Vacuum Gauge | Pirani cold cathode full-scale vacuum gauge |
| Vacuum Range | 1000 mbar to 10^-4 mbar |
| Power Supply | 220 V, 60 Hz, 1.2 KVA |
| Communication | Ethernet |
| Weight | 35 kg |
| Dimensions | 530 × 425 × 461 mm |
Applications
The QAS100 Li DEMS system is designed for in-situ and operando gas analysis in advanced battery systems. Applications shown in the brochure include:
- Quantitative detection of O2 and CO2 evolved from lithium-rich cathodes
- Quantitative detection of O2 and CO2 evolved from high-voltage LiCoO2
- Quantitative detection of O2 and CO2 evolved from sodium-ion cathodes
- In-situ gas analysis for anode materials
- Metal-air battery research
- Electrolyte decomposition studies in lithium-ion batteries
- Research on aqueous Li-ion batteries
- Studies of Li-O2 battery gas evolution behavior
Reference Literature
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Lithium-rich cathodes
ACS Applied Materials & Interfaces 2021, 13, 4062-4071. -
High-voltage LiCoO2
Angewandte Chemie 2021, 133, 27308-27318. -
Ni-rich cathode material
Small 2021, 2104282. -
Sodium ion cathodes
Nature Communications 2021, 12, 5267. -
Aqueous Li-ion batteries
Joule 2022, 6, 399-417. -
Li-O2 battery
ACS Applied Materials & Interfaces 2021, 13, 4062-4071.
